Date of Award

5-2026

Degree Type

Thesis

Degree Name

Honors Thesis

Department

Chemistry

First Advisor

Carl DeAmicis

Second Advisor

Geoffrey Hoops

Abstract

Cyrene is a cellulose-derived molecule that has gained interest in green chemistry as both a solvent and precursor for pharmaceutical intermediates. In this study, biocatalytic and chemical strategies were evaluated for converting Cyrene into these intermediates. Cyrene was carried through variations of a five-step sequence: reduction, reductive amination, esterification, tosylate salt formation, and Lewis-acid mediated acetal opening to generate ring-opened pyranose products (“deoxy sugars” and “deoxy amino sugars”). We successfully synthesized deoxy sugar intermediates; however, the production of stereochemically pure deoxy amino sugar intermediates was limited by unresolved diastereomeric mixtures. These findings highlight the promise of Cyrene as a renewable feedstock and establish a framework for more stereoselective routes of its pharmaceutical synthesis.

Included in

Chemistry Commons

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